ICCAS OpenIR
Solvothermal synthesis and crystal structure of an inorganic-organic hybrid compound [DAMS](2)[CdI4] (DAMS=4-dimethylaminostyryl-1-methyl-pyridinium)
Ren, P; Qin, JG; Chen, CT; Zhang, DQ; Hu, HM
2004-04-01
Source PublicationJOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN1074-1542
Volume34Issue:4Pages:291-294
AbstractAn inorganic-organic hybrid compound [DAMS](2)[CdI4] (DAMS=4-dimethyl-aminostyryl-1-methylpyridinium cation) was synthesized via the solvothermal reaction of equimolar CdI2 and DAMS.I- in a mixture of acetonitrile and H2O (2:1 in volume ratio) at 130degreesC. The product was characterized by X-ray single crystal structure analysis. The crystals of the title compound are triclinic, P-(1) over bar, with a=12.9849(19) Angstrom, b=13.1935(13) Angstrom, c=13.8792(10) Angstrom, alpha=106.798(6)degrees, beta=109.827(6)degrees, gamma=108.206(9)degrees, V=1906.0(4) Angstrom(3), Z=2. The cadmium atom was bonded to 4 iodine atoms to form a distorted tetrahedron, which was surrounded by DAMS cations. There exist pi-pi stacking interaction between the 2 adjacent antiparallelly arrayed DAMS cations.
KeywordSolvothermal Synthesis Inorganic-organic Hybrid Crystal Structure
Indexed BySCI
Language英语
WOS IDWOS:000220601200012
PublisherKLUWER ACADEMIC/PLENUM PUBL
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/81834
Collection中国科学院化学研究所
Corresponding AuthorQin, JG
Affiliation1.Wuhan Univ, Dept Chem, Wuhan 430072, Peoples R China
2.Chinese Acad Sci, Beijing Ctr Crystal Res & Dev, Beijing, Peoples R China
3.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Ren, P,Qin, JG,Chen, CT,et al. Solvothermal synthesis and crystal structure of an inorganic-organic hybrid compound [DAMS](2)[CdI4] (DAMS=4-dimethylaminostyryl-1-methyl-pyridinium)[J]. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,2004,34(4):291-294.
APA Ren, P,Qin, JG,Chen, CT,Zhang, DQ,&Hu, HM.(2004).Solvothermal synthesis and crystal structure of an inorganic-organic hybrid compound [DAMS](2)[CdI4] (DAMS=4-dimethylaminostyryl-1-methyl-pyridinium).JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,34(4),291-294.
MLA Ren, P,et al."Solvothermal synthesis and crystal structure of an inorganic-organic hybrid compound [DAMS](2)[CdI4] (DAMS=4-dimethylaminostyryl-1-methyl-pyridinium)".JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 34.4(2004):291-294.
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