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Michael addition reaction of thiophenol with intramolecular hydrogen bond in aqueous medium
Gao, ZB; Qiu, XP; Guo, HQ; Kang, CQ; Gao, LX
2004-08-01
Source PublicationCHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
ISSN0251-0790
Volume25Issue:8Pages:1471-1473
AbstractThe method of Michael addition reaction of thiophenol with intramolecular hydrogen bond in an aqueous medium was reported. The aqueous reactive medium includes saturated Sodium bicarbonate solution and catalytic amount of tetrabutylammonium bisulfate. 2-Hydroxythiophenol, 2-aininothiophenol, 2-carboxythiophenol, ethyl acrylate and arcylonitrile were selected as model molecules to demonstrate the method. It is found that the reaction can be accomplished rapidly at room temperature with a high yield, and no mercapto-coupling byproduct formed.
KeywordAqueous Reaction Thiophenol Intramolecular Hydrogen Bond Michael Addition
Indexed BySCI
Language英语
WOS IDWOS:000223524600024
PublisherHIGHER EDUCATION PRESS
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/81794
Collection中国科学院化学研究所
Corresponding AuthorGao, LX
AffiliationChinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China
Recommended Citation
GB/T 7714
Gao, ZB,Qiu, XP,Guo, HQ,et al. Michael addition reaction of thiophenol with intramolecular hydrogen bond in aqueous medium[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2004,25(8):1471-1473.
APA Gao, ZB,Qiu, XP,Guo, HQ,Kang, CQ,&Gao, LX.(2004).Michael addition reaction of thiophenol with intramolecular hydrogen bond in aqueous medium.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,25(8),1471-1473.
MLA Gao, ZB,et al."Michael addition reaction of thiophenol with intramolecular hydrogen bond in aqueous medium".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 25.8(2004):1471-1473.
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