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Synthesis and crystal structure of 2,3-dibenzo-1,4,6-triazabicyclo[3.3.1]-2-nonenemonomuriate
Wang, HL; Xue, GL; Xu, YA; Wang, LY; Wang, WL; Hu, HM
2003-07-01
Source PublicationCHINESE JOURNAL OF ORGANIC CHEMISTRY
ISSN0253-2786
Volume23Issue:7Pages:710-713
AbstractThe azo-cycle compound, 2,3-dibenzo-1,4,6-triazabicyclo[3.3.1]-2-nonenemonomuriate, was prepared by condensation of benzil with dienthyltriamine in methanol and in the presence of ZrOCl2, and was characterized by H-1 NMR, IR and UV-vis spectra. Its crystal structure was determined by X-ray diffraction analysis. The crystal belongs to monoclinic system, space group P2(1)/c, cell parameters: a = 1.69341(6) nm, b = 0.77564(3) nm, c = 1.21000(4) nm, beta = 96.1880(10)degrees, Z = 4, D-c = 1.319 g.cm(-3). The compound is a non-planar aza-bicyclo compound with partial unsaturated bonds. The parent hexatomic ring is a chair conformation and the other six-member ring is a half-chair form.
KeywordSynthesis Crystal Structure 2 3-dibenzo-1 4 6-triazabicyclo[3.3.1]-2-nonenemonomuriate
Indexed BySCI
Language英语
WOS IDWOS:000186382600020
PublisherSCIENCE CHINA PRESS
Citation statistics
Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/81394
Collection中国科学院化学研究所
Corresponding AuthorXue, GL
Affiliation1.NW Univ Xian, Dept Chem, Shaanxi Key Lab Physico Inorgan Chem, Xian 710069, Peoples R China
2.Shaanxi Normal Univ, Dept Chem, Xian 710058, Peoples R China
3.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Wang, HL,Xue, GL,Xu, YA,et al. Synthesis and crystal structure of 2,3-dibenzo-1,4,6-triazabicyclo[3.3.1]-2-nonenemonomuriate[J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY,2003,23(7):710-713.
APA Wang, HL,Xue, GL,Xu, YA,Wang, LY,Wang, WL,&Hu, HM.(2003).Synthesis and crystal structure of 2,3-dibenzo-1,4,6-triazabicyclo[3.3.1]-2-nonenemonomuriate.CHINESE JOURNAL OF ORGANIC CHEMISTRY,23(7),710-713.
MLA Wang, HL,et al."Synthesis and crystal structure of 2,3-dibenzo-1,4,6-triazabicyclo[3.3.1]-2-nonenemonomuriate".CHINESE JOURNAL OF ORGANIC CHEMISTRY 23.7(2003):710-713.
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