ICCAS OpenIR
Effects of sodium benzosulfonate on electrochemical polymerization of 2-aminopyridine
Li, X; Lu, RG; Kan, JQ; Xue, HG; Li, YF
2003-08-01
Source PublicationBULLETIN OF ELECTROCHEMISTRY
ISSN0256-1654
Volume19Issue:8Pages:361-366
AbstractPoly-2-aminopyridine is synthesized using cyclic voltammetry between 0 V and 1.10 V (vs. SCE). The electrolytic solution consisted of 0.8 mol. dm(-3) 2- aminopyridine, 0.1 Mol. dm(-3) NaOH and 0.01 mol. dm(-3) sodium benzosulfonate. The film of poly-2-aminopyridine was thickened after adding sodium benzosulfonate. The anodic peak potential and cathodic peak potential of the poly-2-aminopyridine in the 1.0 mmol. dm(-3) CuCl2 solution (pH 3) are influenced by increasing the scan rate from 12 to 480 mVs(-1). Poly-2-aminopyridine has electrochemical reversibility and fast charge transfer characteristic in the 1.0 mmol. dm-3 CuCl2 solution (pH 3). According to the differences between IR spectra of poly-2-aminopyridine and 2-aminopyridine, poly-2-aminopyridine may be head-to-tail structure. XPS have confirmed that Poly-2- aminopyridine can be doped with CuCl2. The SEM image of poly-2-aminopyridine was also given.
Keyword2-aminopyridine Sodium Benzosulfonate Electrochemical Polymerization And Ftir Spectra
Indexed BySCI
Language英语
WOS IDWOS:000185444600004
PublisherCENTRAL ELECTROCHEM RES INST
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/81214
Collection中国科学院化学研究所
Corresponding AuthorKan, JQ
Affiliation1.Yangzhou Univ, Sch Chem & Chem Engn, Yangzhou 225002, Peoples R China
2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Li, X,Lu, RG,Kan, JQ,et al. Effects of sodium benzosulfonate on electrochemical polymerization of 2-aminopyridine[J]. BULLETIN OF ELECTROCHEMISTRY,2003,19(8):361-366.
APA Li, X,Lu, RG,Kan, JQ,Xue, HG,&Li, YF.(2003).Effects of sodium benzosulfonate on electrochemical polymerization of 2-aminopyridine.BULLETIN OF ELECTROCHEMISTRY,19(8),361-366.
MLA Li, X,et al."Effects of sodium benzosulfonate on electrochemical polymerization of 2-aminopyridine".BULLETIN OF ELECTROCHEMISTRY 19.8(2003):361-366.
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