ICCAS OpenIR
Syntheses and X-ray structures of new phenoxy imino compounds
Wang, LY; Sun, WH; Zhang, TZ; He, C
2003-03-01
Source PublicationJOURNAL OF CHEMICAL CRYSTALLOGRAPHY
ISSN1074-1542
Volume33Issue:3Pages:187-193
AbstractFour new phenoxy imino compounds were synthesized, and the solid-state structures of 1-3 were determined by single-crystal X-ray diffraction study, giving crystallographic data as follows. 2-Acetyl-6-[1-(2,6-diisopropylphenylimino)ethyl]-4-methylphenol (1): a = 13.5893(5) Angstrom, b = 10.5781(4) Angstrom, c = 15.6778(4) Angstrom, = 113.1804(18) +/-, P2(1)/c. 2,6-[1-(2,6-=iisopropylphenylimino)ethyl]-4-methylphenol (2).a = 12.1909(5) Angstrom, b = 16.3324(6) Angstrom, c = 15.9456(7) Angstrom, = 96.990(2) +/-, P2(1)/c. 2-Acetyl-6-[ 1-(4-bromine-2,6-dimethylphenylimino)ethyl]-4-methylphenol (3).a = 7.5337(4) Angstrom, b = 10.0457(5) Angstrom, c = 12.6163(4) Angstrom, alpha = 90.139(3) +/-, = 104.003(3)degrees, gamma = 106.485(2)degrees, P - 1. Their molecular structures show that the 2,6- substituted phenyl ring is located approximately orthogonal to the hydroxyphenyl ring with the dihedral angle varying from 85.2degrees to 101.4degrees.
KeywordPhenoxy Imino Compounds Solid-states Structures X-ay Crystal Structures
Indexed BySCI
Language英语
WOS IDWOS:000182463500006
PublisherKLUWER ACADEMIC/PLENUM PUBL
Citation statistics
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/80322
Collection中国科学院化学研究所
Corresponding AuthorSun, WH
Affiliation1.Chinese Acad Sci, State Key Lab Engn Plast, Beijing 100080, Peoples R China
2.Chinese Acad Sci, Inst Chem, Ctr Mol Sci, Beijing 100080, Peoples R China
3.Peking Univ, State Key Lab Rare Earth Mat Chem & Applicat, Nonius BV Demo Lab Xray Diffract, Beijing 100871, Peoples R China
Recommended Citation
GB/T 7714
Wang, LY,Sun, WH,Zhang, TZ,et al. Syntheses and X-ray structures of new phenoxy imino compounds[J]. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,2003,33(3):187-193.
APA Wang, LY,Sun, WH,Zhang, TZ,&He, C.(2003).Syntheses and X-ray structures of new phenoxy imino compounds.JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,33(3),187-193.
MLA Wang, LY,et al."Syntheses and X-ray structures of new phenoxy imino compounds".JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 33.3(2003):187-193.
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