ICCAS OpenIR
Isolation and spectral study of 4-methyl-6,8-dihydroxy-7H-benz[de]anthracen-7-one
Wang, HM; Shi, W; Xu, YK; Wang, P; Chen, W; Liu, Y; Lu, MJ; Pa, JQ
2003-04-01
Source PublicationMAGNETIC RESONANCE IN CHEMISTRY
ISSN0749-1581
Volume41Issue:4Pages:301-303
Abstract4-Methyl-6,8-dihydroxy-7H-benz[de]anthracen-7-one was isolated from the sap of Aloe by column chromatography. Its H-1 and C-13 NMR spectra were completely assigned by utilizing two-dimensional H-1-detected heteronuclear one-bond (HMQC) and multiple-bond (HMBC) chemical shift correlation experiments together with H-1-H-1 COSY and DEPT techniques. These techniques were also valuable in assigning the protons and carbons of those benzanthrone compounds which were previously incompletely reported because of the overlap of proton signals. The molecular structure was elucidated by 2D NMR analysis. The spectral properties (MS, IR and UV) are also presented. Copyright (C) 2003 John Wiley Sons, Ltd.
KeywordNmr H-1 Nmr C-13 Nmr 2d Nmr 4-methyl-6 8-dihydroxy-7h-benz[De]Anthracen-7-one
DOI10.1002/mrc.1148
Indexed BySCI
Language英语
WOS IDWOS:000181855600014
PublisherJOHN WILEY & SONS LTD
Citation statistics
Cited Times:3[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/79968
Collection中国科学院化学研究所
Corresponding AuthorLiu, Y
Affiliation1.Chinese Acad Sci, Inst Chem, State Key Lab Struct Chem Unstable & Stable Speci, Ctr Mol Sci, Beijing 100080, Peoples R China
2.Peking Univ, Ctr Anal & Measurement, Beijing 100871, Peoples R China
Recommended Citation
GB/T 7714
Wang, HM,Shi, W,Xu, YK,et al. Isolation and spectral study of 4-methyl-6,8-dihydroxy-7H-benz[de]anthracen-7-one[J]. MAGNETIC RESONANCE IN CHEMISTRY,2003,41(4):301-303.
APA Wang, HM.,Shi, W.,Xu, YK.,Wang, P.,Chen, W.,...&Pa, JQ.(2003).Isolation and spectral study of 4-methyl-6,8-dihydroxy-7H-benz[de]anthracen-7-one.MAGNETIC RESONANCE IN CHEMISTRY,41(4),301-303.
MLA Wang, HM,et al."Isolation and spectral study of 4-methyl-6,8-dihydroxy-7H-benz[de]anthracen-7-one".MAGNETIC RESONANCE IN CHEMISTRY 41.4(2003):301-303.
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