ICCAS OpenIR
Synthesis and crystal structure of diferrocenyl disulfide
Lu, J; Li, M; Bai, YJ; Hu, HM
2003-03-01
Source PublicationCHINESE JOURNAL OF ORGANIC CHEMISTRY
ISSN0253-2786
Volume23Issue:3Pages:277-280
AbstractDiferrocenyl disulfide was synthesized by the reduction of ferrocenesulfonyl chloride using aluminum iodide as a reducing reagent. The structure was characterized by elemental analysis, IR, H-1 NMR and C-13 NMR spectra. Crystal structure was determined by X-ray diffraction analysis. The crystal data belong to monoclinic space group with unit cell dimensions a = 0.61881(4) nm, b = 1.03231(9) nm, c = 1.39056 (11) nm, beta = 94.179(3)degrees, V = 0.85593(12) nm(3), D-c =1.628 g/cm(3), mu =1.870 mm(-1), F(000) -444, Z =2, R-1 =0.027 and wR(2) =0.0678.
KeywordDiferrocenyl Disulfide Ferrocenesulfonyl Chloride X-ray Diffraction
Indexed BySCI
Language英语
WOS IDWOS:000181587000010
PublisherSCIENCE CHINA PRESS
Citation statistics
Cited Times:2[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/79650
Collection中国科学院化学研究所
Corresponding AuthorLu, J
Affiliation1.NW Univ Xian, Dept Chem, Xian 710069, Peoples R China
2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Lu, J,Li, M,Bai, YJ,et al. Synthesis and crystal structure of diferrocenyl disulfide[J]. CHINESE JOURNAL OF ORGANIC CHEMISTRY,2003,23(3):277-280.
APA Lu, J,Li, M,Bai, YJ,&Hu, HM.(2003).Synthesis and crystal structure of diferrocenyl disulfide.CHINESE JOURNAL OF ORGANIC CHEMISTRY,23(3),277-280.
MLA Lu, J,et al."Synthesis and crystal structure of diferrocenyl disulfide".CHINESE JOURNAL OF ORGANIC CHEMISTRY 23.3(2003):277-280.
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