ICCAS OpenIR
A novel aryl amide-bridged ladderlike polymethylsiloxane synthesized by an amido H-bonding self-assembled template
Tang, HD; Sun, J; Jiang, JQ; Zhou, XS; Hu, TJ; Xie, P; Zhang, R
2002-09-04
Source PublicationJOURNAL OF THE AMERICAN CHEMICAL SOCIETY
ISSN0002-7863
Volume124Issue:35Pages:10482-10488
AbstractA novel soluble aryl amide-bridged ladderlike polymethylsiloxane (A-LPMS) was synthesized by stepwise coupling polymerization on the basis of amido H-bonding self-assembling template from monomer NAr-bis(3-methyldiethoxylsilylpropyl)-[4,4'-oxybis(benzyl amide)]. The monomer was prepared in a high yield by the hydrosilylation reaction of template agent N,N'-diallyl-[4,4'-oxybis(benzyl amide)] with methyldiethoxysilane in the presence of dicyclopentadienylplatinum dichloride (Cp2PtCl2) as catalyst. A variety of techniques including H-1 NMR, C-13 NMR, Si-29 NMR, FTIR, XRD, DSC, and, especially, static and dynamic light scattering and viscosimetry were combined to confirm the presence of the ordered ladderlike structure of polymer A-LPMS.
DOI10.1021/ja025650c
Indexed ByIC ; SCI
Language英语
WOS IDWOS:000177881300045
PublisherAMER CHEMICAL SOC
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/78738
Collection中国科学院化学研究所
Corresponding AuthorZhang, R
AffiliationChinese Acad Sci, Inst Chem, Ctr Mol Sci, State Key Lab Polymer Phys & Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Tang, HD,Sun, J,Jiang, JQ,et al. A novel aryl amide-bridged ladderlike polymethylsiloxane synthesized by an amido H-bonding self-assembled template[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY,2002,124(35):10482-10488.
APA Tang, HD.,Sun, J.,Jiang, JQ.,Zhou, XS.,Hu, TJ.,...&Zhang, R.(2002).A novel aryl amide-bridged ladderlike polymethylsiloxane synthesized by an amido H-bonding self-assembled template.JOURNAL OF THE AMERICAN CHEMICAL SOCIETY,124(35),10482-10488.
MLA Tang, HD,et al."A novel aryl amide-bridged ladderlike polymethylsiloxane synthesized by an amido H-bonding self-assembled template".JOURNAL OF THE AMERICAN CHEMICAL SOCIETY 124.35(2002):10482-10488.
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