ICCAS OpenIR
Synthesis of phenyl/amino-capped tetraaniline by chemical and electrochemical methods
Sun, ZC; Kuang, L; Jing, XB; Wang, XH; Li, J; Wang, FS
2002-03-01
Source PublicationCHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
ISSN0251-0790
Volume23Issue:3Pages:496-499
AbstractPhenyl/amino-capped tetraaniline was prepared by chemical oxidation coupling and electrochemical cyclic voltammetry methods. The MacDiarmid's method of oxidation coupling was improved. The aqueous HCl was replaced with a mixture solution of HCl and acetone and (NH4)(2)S(2)O(0)8 was used as oxidant instead of FeCl3. The reaction displays a higher yield and the product tetraaniline has a higher purity owing to the improvement. In the mixture solution system, tetraaniline can be synthesized by electrochemical cyclic voltammetry method. The mechanism by which tetraaniline was prepared from p-amino diphenylamine was proposed. The product was characterized by MALDI-TOF MS and FTIR.
KeywordPhenyl/amino-capped Tetraaniline Chemical Oxidation Coupling Electrochemical Cyclic Voltammtry Method
Indexed BySCI
Language英语
WOS IDWOS:000175465700041
PublisherHIGHER EDUCATION PRESS
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/78216
Collection中国科学院化学研究所
Corresponding AuthorKuang, L
Affiliation1.Hainan Entry Exit Inspect & Quarantine, Haikou 570311, Peoples R China
2.Chinese Acad Sci, Polymer Chem Lab, State Key Lab Polymer Phys & Chem, Changchun 130022, Peoples R China
3.Chinese Acad Sci, Changchun Inst Appl Chem, China Petrochem Corp, Changchun 130022, Peoples R China
Recommended Citation
GB/T 7714
Sun, ZC,Kuang, L,Jing, XB,et al. Synthesis of phenyl/amino-capped tetraaniline by chemical and electrochemical methods[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2002,23(3):496-499.
APA Sun, ZC,Kuang, L,Jing, XB,Wang, XH,Li, J,&Wang, FS.(2002).Synthesis of phenyl/amino-capped tetraaniline by chemical and electrochemical methods.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,23(3),496-499.
MLA Sun, ZC,et al."Synthesis of phenyl/amino-capped tetraaniline by chemical and electrochemical methods".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 23.3(2002):496-499.
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