ICCAS OpenIR
Synthesis and characterization of a novel soluble reactive ladder-like polysilsesquioxane with side-chain 2-(4-chloromethyl phenyl) ethyl groups
Liu, CQ; Liu, Y; Xie, P; Dai, DR; Zhang, RB
2001-08-01
Source PublicationPOLYMERS FOR ADVANCED TECHNOLOGIES
ISSN1042-7147
Volume12Issue:8Pages:475-481
AbstractA new kind of soluble structure-ordered ladder-like polysilsesquioxane with reactive side-chain 2-(4-chloromethyl phenyl) ethyl groups (L) was first synthesized by stepwise coupling polymerization. The monomer, 2-(4-chloromethyl phenyl) ethyltrichlorosilane (M), was synthesized successfully by hydrosilylation reaction with dicyclopentadienylplatinum(II) chloride (CP2PtCl2) catalyst. Monomer and polymer structures were characterized by FT-IR, H-1-NMR, C-13-NMR, Si-29-NMR, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), vapor pressure osmometry (VPO) and X-ray diffraction (XRD) This novel reactive ladder-like polymer has promise potential applications as initiator for atom transfer radical polymerization, and as precursor for a variety of advanced functional polymers. Copyright (C) 2001 John Wiley & Sons, Ltd.
KeywordLadder-like Polysilsesquioxane Stepwise Coupling Polymerization Hydrosilylation 2-(4-chloro-mEthyl Phenyl) Ethyl Groups Characterization
Indexed BySCI
Language英语
WOS IDWOS:000170793200004
PublisherJOHN WILEY & SONS LTD
Citation statistics
Cited Times:9[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/77958
Collection中国科学院化学研究所
Corresponding AuthorZhang, RB
Affiliation1.Chinese Acad Sci, Polymer Chem Lab, Beijing 100080, Peoples R China
2.Chinese Acad Sci, Inst Chem, China Petrochem Corp, Ctr Mol Sci, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Liu, CQ,Liu, Y,Xie, P,et al. Synthesis and characterization of a novel soluble reactive ladder-like polysilsesquioxane with side-chain 2-(4-chloromethyl phenyl) ethyl groups[J]. POLYMERS FOR ADVANCED TECHNOLOGIES,2001,12(8):475-481.
APA Liu, CQ,Liu, Y,Xie, P,Dai, DR,&Zhang, RB.(2001).Synthesis and characterization of a novel soluble reactive ladder-like polysilsesquioxane with side-chain 2-(4-chloromethyl phenyl) ethyl groups.POLYMERS FOR ADVANCED TECHNOLOGIES,12(8),475-481.
MLA Liu, CQ,et al."Synthesis and characterization of a novel soluble reactive ladder-like polysilsesquioxane with side-chain 2-(4-chloromethyl phenyl) ethyl groups".POLYMERS FOR ADVANCED TECHNOLOGIES 12.8(2001):475-481.
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