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Synthesis and properties of polysiloxane containing N,N '-bis(diphenylsilyl)tetraphenylcyclodisilazane
Zhou, N; Zhang, ZJ; Xu, CH; Xie, ZM
2001-10-24
Source PublicationJOURNAL OF APPLIED POLYMER SCIENCE
ISSN0021-8995
Volume82Issue:4Pages:929-933
AbstractA new kind of polysiloxane containing N,N ' -bis(diphenylsilyl)tetraphenyl-cyclodisilazane was prepared by the anionic polymerization with a "Seed solution" as initiator. The synthesis of monomers N,N ' -bis(hydroxydiphenylsilyl)tetraphenylcyclodisilazane (BHPTPC), N,N ' -bis(chlorodiphenyisilyl)tetraphenylcyclodisilazane (BCPTPC), and 1,3-dichloro-1,1,3,3-tetraphenyldisilazane (DCTPS) are all reported in this study, The synthesized polysiloxane containing N,N ' -bis(diphenylsilyl)tetraphenylcyclodisilazane was characterized by H-1-NMR, Si-29-NMR, gel permeation chromatography (GPC), and intrinsic viscosity. The thermal stability of the polysiloxane was studied by isothermal gravimetric analysis (IGA). The results demonstrated that the synthesized polysiloxane containing N,N ' -bis(diphenylsilyl)tetraphenylcyclodisilazane had excellent thermal stability. (C) 2001 John Wiley & Sons, Inc.
KeywordPolysiloxane Synthesis Thermal Stability n n '-bis(Diphenylsilyl)Tetraphenylcyclodisilazane
Indexed BySCI
Language英语
WOS IDWOS:000170509000018
PublisherJOHN WILEY & SONS INC
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/77808
Collection中国科学院化学研究所
Corresponding AuthorXie, ZM
AffiliationChinese Acad Sci, Inst Chem, Ctr Mol Sci, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Zhou, N,Zhang, ZJ,Xu, CH,et al. Synthesis and properties of polysiloxane containing N,N '-bis(diphenylsilyl)tetraphenylcyclodisilazane[J]. JOURNAL OF APPLIED POLYMER SCIENCE,2001,82(4):929-933.
APA Zhou, N,Zhang, ZJ,Xu, CH,&Xie, ZM.(2001).Synthesis and properties of polysiloxane containing N,N '-bis(diphenylsilyl)tetraphenylcyclodisilazane.JOURNAL OF APPLIED POLYMER SCIENCE,82(4),929-933.
MLA Zhou, N,et al."Synthesis and properties of polysiloxane containing N,N '-bis(diphenylsilyl)tetraphenylcyclodisilazane".JOURNAL OF APPLIED POLYMER SCIENCE 82.4(2001):929-933.
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