ICCAS OpenIR
Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O
Bian, ZQ; Li, FY; Jin, LP; Guo, JQ; Wang, KZ; Yang, MS
2001-10-03
Source PublicationJOURNAL OF MOLECULAR STRUCTURE
ISSN0022-2860
Volume597Issue:1-3Pages:121-127
AbstractThe structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) was determined by single crystal X-ray diffraction. The crystal is triclinic, space group P1 with cell dimensions of a = 0.80821(13) nm, b = 1.08777(13) nm, c = 1.09263(13) nm, alpha = 113.045(50)degrees, beta =95.428(11)degrees, gamma = 91.162(12)degrees, V= 0.8782(2) nm(3), Z= 2, mu,(MoK alpha) = 0.107 nm(-1), D-x = 1.382 g cm(-3). The ligand L has an intramolecular hydrogen bond [O(7)-(HO)-O-...(5)] resulting in the formation of a seven-membered ring. The isolation and characterization of Ln(2)L(3)(SCN)(3).2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3).2H(2)O are reported. (C) 2001 Elsevier Science B.V. All rights reserved.
KeywordSynthesis Rare Earth Complex X-ray Crystallography N-(Oxabutyl-2-ene Acid)-2 3-benzo-10-aza-1 4 7 13-tetraoxacyclopentadeca-2-ene
Indexed BySCI
Language英语
WOS IDWOS:000171335000014
PublisherELSEVIER SCIENCE BV
Citation statistics
Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/77248
Collection中国科学院化学研究所
Corresponding AuthorJin, LP
Affiliation1.Beijing Normal Univ, Dept Chem, Beijing 100875, Peoples R China
2.Chinese Acad Sci, Inst Chem, Beijing 100084, Peoples R China
Recommended Citation
GB/T 7714
Bian, ZQ,Li, FY,Jin, LP,et al. Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O[J]. JOURNAL OF MOLECULAR STRUCTURE,2001,597(1-3):121-127.
APA Bian, ZQ,Li, FY,Jin, LP,Guo, JQ,Wang, KZ,&Yang, MS.(2001).Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O.JOURNAL OF MOLECULAR STRUCTURE,597(1-3),121-127.
MLA Bian, ZQ,et al."Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O".JOURNAL OF MOLECULAR STRUCTURE 597.1-3(2001):121-127.
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