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| Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O | |
| Bian, ZQ; Li, FY; Jin, LP; Guo, JQ; Wang, KZ; Yang, MS | |
| 2001-10-03 | |
| Source Publication | JOURNAL OF MOLECULAR STRUCTURE
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| ISSN | 0022-2860 |
| Volume | 597Issue:1-3Pages:121-127 |
| Abstract | The structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) was determined by single crystal X-ray diffraction. The crystal is triclinic, space group P1 with cell dimensions of a = 0.80821(13) nm, b = 1.08777(13) nm, c = 1.09263(13) nm, alpha = 113.045(50)degrees, beta =95.428(11)degrees, gamma = 91.162(12)degrees, V= 0.8782(2) nm(3), Z= 2, mu,(MoK alpha) = 0.107 nm(-1), D-x = 1.382 g cm(-3). The ligand L has an intramolecular hydrogen bond [O(7)-(HO)-O-...(5)] resulting in the formation of a seven-membered ring. The isolation and characterization of Ln(2)L(3)(SCN)(3).2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3).2H(2)O are reported. (C) 2001 Elsevier Science B.V. All rights reserved. |
| Keyword | Synthesis Rare Earth Complex X-ray Crystallography N-(Oxabutyl-2-ene Acid)-2 3-benzo-10-aza-1 4 7 13-tetraoxacyclopentadeca-2-ene |
| Indexed By | SCI |
| Language | 英语 |
| WOS ID | WOS:000171335000014 |
| Publisher | ELSEVIER SCIENCE BV |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.iccas.ac.cn/handle/121111/77248 |
| Collection | 中国科学院化学研究所 |
| Corresponding Author | Jin, LP |
| Affiliation | 1.Beijing Normal Univ, Dept Chem, Beijing 100875, Peoples R China 2.Chinese Acad Sci, Inst Chem, Beijing 100084, Peoples R China |
| Recommended Citation GB/T 7714 | Bian, ZQ,Li, FY,Jin, LP,et al. Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O[J]. JOURNAL OF MOLECULAR STRUCTURE,2001,597(1-3):121-127. |
| APA | Bian, ZQ,Li, FY,Jin, LP,Guo, JQ,Wang, KZ,&Yang, MS.(2001).Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O.JOURNAL OF MOLECULAR STRUCTURE,597(1-3),121-127. |
| MLA | Bian, ZQ,et al."Crystal structure of N-(oxabutyl-2-ene acid)-2,3-benzo-10-aza-1,4,7,13-tetraoxacyclopentadeca-2-ene (L) and characterization of Ln(2)L(3)(SCN)(3)center dot 2H(2)O (Ln = La, Eu, Dy) and Eu2L3(NO3)(3)center dot 2H(2)O".JOURNAL OF MOLECULAR STRUCTURE 597.1-3(2001):121-127. |
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