ICCAS OpenIR
Resolution of optical isomers of alpha-hydroxy-acetones by high resolution gas chromatography on chiral stationary phase
Zhang, YQ; Shi, XY; Fu, RN; Zhang, HB; Ling, Y; Zuo, XB; Liu, HF
2001-03-01
Source PublicationCHINESE JOURNAL OF ANALYTICAL CHEMISTRY
ISSN0253-3820
Volume29Issue:3Pages:336-338
AbstractUsing the cyclodextrin bonded polysiloxane (bikis[(2,6-di-O-pentyl-3-O-hex-6-O-enyl -di-O-pentyl-3-O-methyl)-beta -cyclodextrm-polysiloxane])) as gas chromatographic stationary phase, a-hydroxy-acetones were separated and the values of the enantiomeric excess(e. e) of 3-hydroxy-2-butanone were determined. the results showed that the high resolution gas chromatography (HRGC) using the chiral gas chromatographic stationary phase could determine the productive rate of the asymmetric hydrogenaton reaction and evaluate the enantoselectivity of the catalyst system.
KeywordHigh Resolution Gas Chromatography Chiral Stationary Phase 2 Bikis [(2 6-di-o-pentyl-3-o-trifluoroacetyl-beta-cyclodextrin 6-di-o-pentyl-3-o-hex-6-o-enyl)-pentakis (2 6 -di-o-pentyl-3-o-methyl)-beta-cyclodextrin-polysiloxane]
Indexed BySCI
Language英语
WOS IDWOS:000167761200025
PublisherFENXI HUAXUE
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/77036
Collection中国科学院化学研究所
Corresponding AuthorFu, RN
Affiliation1.Beijing Inst Technol, Sch Chem Engn & Mat Sci, Beijing 100081, Peoples R China
2.Chinese Acad Sci, Inst Chem, Polymer Chem Lab, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Zhang, YQ,Shi, XY,Fu, RN,et al. Resolution of optical isomers of alpha-hydroxy-acetones by high resolution gas chromatography on chiral stationary phase[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2001,29(3):336-338.
APA Zhang, YQ.,Shi, XY.,Fu, RN.,Zhang, HB.,Ling, Y.,...&Liu, HF.(2001).Resolution of optical isomers of alpha-hydroxy-acetones by high resolution gas chromatography on chiral stationary phase.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,29(3),336-338.
MLA Zhang, YQ,et al."Resolution of optical isomers of alpha-hydroxy-acetones by high resolution gas chromatography on chiral stationary phase".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 29.3(2001):336-338.
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