ICCAS OpenIR
Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane
Liu, CQ; Zhao, HT; Xie, P; Zhang, RB
2000-08-01
Source PublicationJOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY
ISSN0887-624X
Volume38Issue:15Pages:2702-2710
AbstractA novel soluble, reactive ladderlike 4,4'-phenylene ether-bridged polyvinyl-siloxane (L) was synthesized successfully for the first time by a stepwise coupling polymerization (SCP) including hydrolysis and polycondensation. The monomer, 4,4'-bis(vinyldimethoxysilyl )phenylene ether (M), was synthesized by Grignard reaction. The structures of the monomer and the polymer were characterized by infrared spectrometry (IR), nuclear magnetic resonance (H-1 NMR, C-13 NMR, Si-29 NMR), mass spectrometry (MS), differential scanning calorimetry (DSC), X-ray diffration (XRD), and gel permeation chromatography (GPC). It is proposed from the characterization data that the polymer possesses an ordered ladderlike structure. (C) 2000 John Wiley & Sons, Inc.
KeywordGrignard Reaction Hydrolysis Polycondensation Characterization Ladderlike 4 4 ' -phenylene Ether-bridged Polyvinylsiloxane
Indexed BySCI
Language英语
WOS IDWOS:000088202300010
PublisherJOHN WILEY & SONS INC
Citation statistics
Cited Times:25[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/75714
Collection中国科学院化学研究所
Corresponding AuthorZhang, RB
AffiliationChinese Acad Sci, PCLCC, Ctr Mol Sci, Inst Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Liu, CQ,Zhao, HT,Xie, P,et al. Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane[J]. JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY,2000,38(15):2702-2710.
APA Liu, CQ,Zhao, HT,Xie, P,&Zhang, RB.(2000).Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane.JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY,38(15),2702-2710.
MLA Liu, CQ,et al."Synthesis and characterization of a novel reactive ladderlike 4,4 '-phenylene ether-bridged polyvinylsiloxane".JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY 38.15(2000):2702-2710.
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