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New bisdithiolene metal complex of the 2-thioxo-1,3-dithiole-4,5-dithiolato(dmit) ligand. Preparation, structure and physical properties
Zhang, QC; Wu, PJ; Sun, SQ; Zhu, DB; Xong, M; Ma, ZS; Shi, NC
1998-12-04
Source PublicationSYNTHETIC METALS
ISSN0379-6779
Volume98Issue:2Pages:103-106
AbstractThe complex HMEDA[Ni(dmit)(2)](2)I (HMEDA = Hexamethylethylenediammonium) has been prepared. A single X-ray crystal structure analysis reveals that there are short S ... S contacts between Ni(dmit)(2) dimmers. The monoclinic system, space group p2/n, has cell dimensions: a = 11.710(3) Angstrom, b = 22.559(5) Angstrom, c = 7.374(2) Angstrom, beta = 93.000(3)(0), V = 1945.3(8) Angstrom(3), z = 4. Full-matrix least-squares refinement, based on 2989 reflections converged at R = 0.0686. The conductivity of this salt at room temperature is 0.1 S cm(-1) and it shows semiconducting behavior from 20 to 300 K. (C) 1998 Elsevier Science S.A. All rights reserved.
KeywordNickel Complexes Dithiolate Complexes Electrical Conductivity Crystal Structure Synthesis
Indexed BySCI
Language英语
WOS IDWOS:000077636400004
PublisherELSEVIER SCIENCE SA
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Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/74546
Collection中国科学院化学研究所
Corresponding AuthorZhu, DB
Affiliation1.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
2.China Univ Geosci, Xray Lab, Beijing 100083, Peoples R China
Recommended Citation
GB/T 7714
Zhang, QC,Wu, PJ,Sun, SQ,et al. New bisdithiolene metal complex of the 2-thioxo-1,3-dithiole-4,5-dithiolato(dmit) ligand. Preparation, structure and physical properties[J]. SYNTHETIC METALS,1998,98(2):103-106.
APA Zhang, QC.,Wu, PJ.,Sun, SQ.,Zhu, DB.,Xong, M.,...&Shi, NC.(1998).New bisdithiolene metal complex of the 2-thioxo-1,3-dithiole-4,5-dithiolato(dmit) ligand. Preparation, structure and physical properties.SYNTHETIC METALS,98(2),103-106.
MLA Zhang, QC,et al."New bisdithiolene metal complex of the 2-thioxo-1,3-dithiole-4,5-dithiolato(dmit) ligand. Preparation, structure and physical properties".SYNTHETIC METALS 98.2(1998):103-106.
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