ICCAS OpenIR
Monosubstituted arylimido hexamolybdates containing pendant amino groups: synthesis and structural characterization
Zhu, Yi1; Xiao, Zicheng1,2; Wang, Longsheng2; Yin, Panchao2; Hao, Jian2; Wei, Yongge1,2,3; Wang, Yuan1
2011-07-28
Source PublicationDALTON TRANSACTIONS
ISSN1477-9226
Volume40Issue:28Pages:7304-7309
AbstractThree novel rigid-rod conjugated organic-POM hybrids (1, 2 and 3) containing pendant amino terminus, with different rod lengths and different substituents on the rod, have been respectively synthesized via one-pot reaction of hexamolybdate and the corresponding aromatic diamine (for 1 and 2) and reaction of octamolybdate and the corresponding aromatic diamine dihydrochloride (for 3) with N,N'-dicyclohexylcarbodiimide (DCC) as a dehydrating agent. These complexes have been characterized by UV/Vis, IR, (1)H NMR, ESI and single-crystal X-ray diffraction techniques. The influences of the rod length and substituents on the properties of these compounds have been systematically investigated, which provide necessary information for further preparations of complicated hybrid materials via reactions with pendant amino groups.
DOI10.1039/c1dt10168d
Indexed BySCI
Language英语
WOS IDWOS:000292987200005
PublisherROYAL SOC CHEMISTRY
Citation statistics
Cited Times:10[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/73908
Collection中国科学院化学研究所
Corresponding AuthorWei, Yongge
Affiliation1.Peking Univ, Dept Chem, State Key Lab Struct Chem Unstable & Stable Speci, Coll Chem & Mol Engn, Beijing 100871, Peoples R China
2.Tsinghua Univ, Dept Chem, Beijing 100084, Peoples R China
3.Beijing Inst Technol, Key Lab Cluster Sci, Minist Educ China, Beijing 100081, Peoples R China
Recommended Citation
GB/T 7714
Zhu, Yi,Xiao, Zicheng,Wang, Longsheng,et al. Monosubstituted arylimido hexamolybdates containing pendant amino groups: synthesis and structural characterization[J]. DALTON TRANSACTIONS,2011,40(28):7304-7309.
APA Zhu, Yi.,Xiao, Zicheng.,Wang, Longsheng.,Yin, Panchao.,Hao, Jian.,...&Wang, Yuan.(2011).Monosubstituted arylimido hexamolybdates containing pendant amino groups: synthesis and structural characterization.DALTON TRANSACTIONS,40(28),7304-7309.
MLA Zhu, Yi,et al."Monosubstituted arylimido hexamolybdates containing pendant amino groups: synthesis and structural characterization".DALTON TRANSACTIONS 40.28(2011):7304-7309.
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