ICCAS OpenIR
Synthesis of a Novel Series of Propargyloxyphenyl Maleimides and Their Characterization as Thermal-Resistance Resins
Liu, Feng; Liu, Jinge; Zhao, Tong
2010-03-05
Source PublicationJOURNAL OF APPLIED POLYMER SCIENCE
ISSN0021-8995
Volume115Issue:5Pages:3103-3109
AbstractNovel thermosetting monomers possessing both maleimide and propargyl groups were first designed and synthesized. The monomers included N-(2-propargyloxyphenyl) maleimide (2-PPM), N-(3-propargyloxyphenyl) maleimide (3-PPM), and N-(4-propargyloxyphenyl) maleimide (4-PPM), and their structures were confirmed with Fourier transform infrared (FTIR) spectroscopy, (1)H-NMR, and elemental analysis. The cure behaviors of these monomers were characterized with differential scanning calorimetry and FTIR spectroscopy, and the results indicated that the monomers had a broader processing window than normal bismaleimide (BMI) resins. The thermal properties of the cured monomers were characterized with thermogravimetric analysis and dynamic mechanical analysis. The 5% mass loss temperatures of the cured monomers were high (ca. 400 degrees C), and the glass-transition temperatures of cured 2-PPM, 3-PPM, and 4-PPM were 386, 373, and 387 degrees C, respectively, which were much higher than those of typical commercial blended BMI resins. (C) 2009 Wiley Periodicals, Inc. J Appl Polym Sci 115: 3103-3109, 2010
KeywordAddition Polymerization Monomers Thermal Properties
DOI10.1002/app.31174
Indexed BySCI
Language英语
WOS IDWOS:000274114000070
PublisherJOHN WILEY & SONS INC
Citation statistics
Cited Times:9[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/70962
Collection中国科学院化学研究所
Corresponding AuthorZhao, Tong
AffiliationChinese Acad Sci, Inst Chem, Beijing 100190, Peoples R China
Recommended Citation
GB/T 7714
Liu, Feng,Liu, Jinge,Zhao, Tong. Synthesis of a Novel Series of Propargyloxyphenyl Maleimides and Their Characterization as Thermal-Resistance Resins[J]. JOURNAL OF APPLIED POLYMER SCIENCE,2010,115(5):3103-3109.
APA Liu, Feng,Liu, Jinge,&Zhao, Tong.(2010).Synthesis of a Novel Series of Propargyloxyphenyl Maleimides and Their Characterization as Thermal-Resistance Resins.JOURNAL OF APPLIED POLYMER SCIENCE,115(5),3103-3109.
MLA Liu, Feng,et al."Synthesis of a Novel Series of Propargyloxyphenyl Maleimides and Their Characterization as Thermal-Resistance Resins".JOURNAL OF APPLIED POLYMER SCIENCE 115.5(2010):3103-3109.
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