ICCAS OpenIR
Ethynyl Aromatic Siliconhybridized Resin: Synthesis, Characterizations, and Thermal Properties
Yang, Ming1,2; Shi, Song3; Wang, Mingcun1; Wang, Yuhui3; Luo, Zhenhua1; Feng, Zhihai3; Zhao, Tong1
2010-07-15
Source PublicationJOURNAL OF APPLIED POLYMER SCIENCE
ISSN0021-8995
Volume117Issue:2Pages:714-719
AbstractA novel silicon-containing resin (ESA resin) was successfully synthesized by the condensation reaction of lithium arylacetylide with chlorosilane in high yields. The resin was characterized by the techniques of FTIR, (29)Si-NMR, and gel permeation chromatography. Thermal cure process was monitored by DSC and FTIR methods. This resin could melt at around 100 degrees C and thermally cured at 200-250 degrees C with low exothermal enthalpy. Owing to the high aryl groups containing and the complete crosslinking of ethynyl groups, the cured ESA resin exhibited excellent thermal stability and high char yield. The decomposition temperature T(d5) of the cured resin was at 510 degrees C, and the residue yield at 900 degrees C was 82.9% in N(2). (C) 2010 Wiley Periodicals, Inc. J Appl Polym Sci 117: 714-719, 2010
KeywordEthynyl Aromatic Silicones Thermosets Thermal Properties
DOI10.1002/app.31237
Indexed BySCI
Language英语
WOS IDWOS:000278162600011
PublisherJOHN WILEY & SONS INC
Citation statistics
Cited Times:3[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/69422
Collection中国科学院化学研究所
Corresponding AuthorZhao, Tong
Affiliation1.Chinese Acad Sci, Inst Chem, Lab Adv Polymer Mat, Beijing 100190, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Aerosp Res Inst Mat & Proc Technol, Natl Key Lab Adv Funct Composite Mat, Beijing 100076, Peoples R China
Recommended Citation
GB/T 7714
Yang, Ming,Shi, Song,Wang, Mingcun,et al. Ethynyl Aromatic Siliconhybridized Resin: Synthesis, Characterizations, and Thermal Properties[J]. JOURNAL OF APPLIED POLYMER SCIENCE,2010,117(2):714-719.
APA Yang, Ming.,Shi, Song.,Wang, Mingcun.,Wang, Yuhui.,Luo, Zhenhua.,...&Zhao, Tong.(2010).Ethynyl Aromatic Siliconhybridized Resin: Synthesis, Characterizations, and Thermal Properties.JOURNAL OF APPLIED POLYMER SCIENCE,117(2),714-719.
MLA Yang, Ming,et al."Ethynyl Aromatic Siliconhybridized Resin: Synthesis, Characterizations, and Thermal Properties".JOURNAL OF APPLIED POLYMER SCIENCE 117.2(2010):714-719.
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