ICCAS OpenIR
Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework
Yang, Sihai1; Li, Guobao1; Liu, Wei2; Wang, Wei2; Yan, Zhimin3; Huang, Yining3; Liao, Fuhui1; Lin, Jianhua1
2009-06-15
Source PublicationINORGANIC CHEMISTRY
ISSN0020-1669
Volume48Issue:12Pages:5449-5453
Abstract(NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] (1) has been synthesized under hydrothermal conditions. The structure, the composition, and the thermal stability of 1 were determined by single-crystal X-ray diffraction; inductively coupled plasma-optical emission spectroscopy; IR spectroscopy; elemental analysis; thermogravimetric analysis-differential scanning calorimetry-mass spectrometry; and solid-state H-1, P-31, and F-19 NMR, and the phase purity of the bulk sample was checked by powder X-ray diffraction. Complex 1 is a fluorotitanophosphate having a unique lamella framework with both TiO5F octahedra and PO3OH tetrahedra on the surface of the layer, which leads to two different hydrogen bondings involving both P-OH and Ti-F groups.
DOI10.1021/ic900504m
Indexed BySCI
Language英语
WOS IDWOS:000266809200047
PublisherAMER CHEMICAL SOC
Citation statistics
Cited Times:6[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/66832
Collection中国科学院化学研究所
Corresponding AuthorLi, Guobao
Affiliation1.Peking Univ, BNLMS, State Key Lab Rare Earth Mat Chem & Applicat, Coll Chem & Mol Engn, Beijing 100871, Peoples R China
2.Lanzhou Univ, State Key Lab Appl Organ Chem, Coll Chem & Chem Engn, Lanzhou 730000, Gansu, Peoples R China
3.Univ Western Ontario, Dept Chem, London, ON N6A 5B7, Canada
Recommended Citation
GB/T 7714
Yang, Sihai,Li, Guobao,Liu, Wei,et al. Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework[J]. INORGANIC CHEMISTRY,2009,48(12):5449-5453.
APA Yang, Sihai.,Li, Guobao.,Liu, Wei.,Wang, Wei.,Yan, Zhimin.,...&Lin, Jianhua.(2009).Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework.INORGANIC CHEMISTRY,48(12),5449-5453.
MLA Yang, Sihai,et al."Synthesis and Characterization of a Fluorotitanophosphate (NH4)(0.16)K-1.84[Ti2F2(PO4)(2)(PO3OH)] with a Unique Lamella Framework".INORGANIC CHEMISTRY 48.12(2009):5449-5453.
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