ICCAS OpenIR
Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes
Ding, Jiapei; Tao, Zhiqiang; Zuo, Xiaobiao; Fan, Lin; Yang, Shiyong
2009-06-01
Source PublicationPOLYMER BULLETIN
ISSN0170-0839
Volume62Issue:6Pages:829-841
AbstractNovel epoxy resin modifiers, DOPO-TMDS and DOPO-DMDP were synthesized by addition reaction of divinylsiloxane with 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO). Halogen-free flame retardant epoxy resins were obtained through modification of o-cresol novolac epoxy resin cured by phenol novolac resin using DOPO-TMDS and DOPO-DMDP which were characterized by (1)H NMR, (13)C NMR, (31)P NMR and FT-IR measurements. Effects of the phosphorus-containing siloxanes on thermal stabilities, mechanical properties and flame retardant properties of the epoxy resins were investigated. The cured epoxy resins exhibited better mechanical properties and greatly improved flame retardant properties due to the presence of phosphorus-containing siloxanes. The cured epoxy resins with phosphorus loading of 2.0 wt% showed LOI values of 32-33 and achieved UL94V-0 ratings.
KeywordEpoxy Flame Retardancy Mechanical Properties Phosphorus Silicon
DOI10.1007/s00289-009-0052-0
Indexed BySCI
Language英语
WOS IDWOS:000266262700009
PublisherSPRINGER
Citation statistics
Cited Times:33[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/66260
Collection中国科学院化学研究所
Corresponding AuthorTao, Zhiqiang
AffiliationChinese Acad Sci, Inst Chem, Lab Adv Polymer Mat, Beijing 100190, Peoples R China
Recommended Citation
GB/T 7714
Ding, Jiapei,Tao, Zhiqiang,Zuo, Xiaobiao,et al. Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes[J]. POLYMER BULLETIN,2009,62(6):829-841.
APA Ding, Jiapei,Tao, Zhiqiang,Zuo, Xiaobiao,Fan, Lin,&Yang, Shiyong.(2009).Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes.POLYMER BULLETIN,62(6),829-841.
MLA Ding, Jiapei,et al."Preparation and properties of halogen-free flame retardant epoxy resins with phosphorus-containing siloxanes".POLYMER BULLETIN 62.6(2009):829-841.
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