ICCAS OpenIR
Shape-controlled synthesis of palladium nanocrystals by microwave irradiation
Yu, Yanchun1; Zhao, Yanxi1; Huang, Tao1; Liu, Hanfan1,2
2009-12-01
Source PublicationPURE AND APPLIED CHEMISTRY
ISSN0033-4545
Volume81Issue:12Pages:2377-2385
AbstractThe controlled synthesis of Pd icosahedra in tetraethylene glycol (TEG) with H(2)PdCl(4) as a precursor and poly(vinylpyrrolidone) (PVP) as a stabilizer in the presence of an appropriate amount of KOH under microwave irradiation was demonstrated. TEG served as both solvent and reducing agent, and stable Pd icosahedra with uniform sizes and well-defined shapes could be prepared in a yield of over 90 % by microwave heating for 60 s. The sizes of Pd icosahedra can be well controlled by adjusting the concentration of the precursor H(2)PdCl(4).
KeywordIcosahedra Microwave Polyol Process Nanoparticles Palladium Tetraethylene Glycol
DOI10.1351/PAC-CON-08-11-22
Indexed BySCI ; ISTP
Language英语
WOS IDWOS:000273206200015
PublisherINT UNION PURE APPLIED CHEMISTRY
Citation statistics
Cited Times:34[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.iccas.ac.cn/handle/121111/66036
Collection中国科学院化学研究所
Corresponding AuthorHuang, Tao
Affiliation1.S Cent Univ Nationalities, Coll Chem & Mat Sci, Wuhan 430074, Peoples R China
2.Chinese Acad Sci, Inst Chem, Beijing 100080, Peoples R China
Recommended Citation
GB/T 7714
Yu, Yanchun,Zhao, Yanxi,Huang, Tao,et al. Shape-controlled synthesis of palladium nanocrystals by microwave irradiation[J]. PURE AND APPLIED CHEMISTRY,2009,81(12):2377-2385.
APA Yu, Yanchun,Zhao, Yanxi,Huang, Tao,&Liu, Hanfan.(2009).Shape-controlled synthesis of palladium nanocrystals by microwave irradiation.PURE AND APPLIED CHEMISTRY,81(12),2377-2385.
MLA Yu, Yanchun,et al."Shape-controlled synthesis of palladium nanocrystals by microwave irradiation".PURE AND APPLIED CHEMISTRY 81.12(2009):2377-2385.
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